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论文摘要

一种简单的溶胶-凝胶法制备二氧化锆介质层

Zirconium Dioxide Prepared with a Simple Sol-Gel Method

作者:李国安(四川大学物理科学与技术学院);杜惊雷(四川大学物理科学与技术学院);Leander Schulz(四川大学物理科学与技术学院)

Author:LI Guo-An(College of Physical and Technology, Sichuan University);DU Jing-Lei(College of Physical and Technology, Sichuan University);Leander Schulz(College of Physical and Technology, Sichuan University)

收稿日期:2016-03-01          年卷(期)页码:2016,53(4):843-846

期刊名称:四川大学学报: 自然科学版

Journal Name:Journal of Sichuan University (Natural Science Edition)

关键字:二氧化锆;溶胶-凝胶法;电介质

Key words:zirconium dioxide; sol-gel method;dielectric

基金项目:国家自然科学基金,项目编号:61404088

中文摘要

在电子产业中,能够进行低压操作以及能够在非常薄的薄层上进行器件设计的材料备受关注。并且,这些材料需要使用方法简单、快速、可靠。作者提出一种简单且快速可靠的沉积高k 二氧化锆介电层的方法。整个过程从原来常规过程的140分钟缩短到10分钟。这种改进的方法在操作流程方面有显著的提升。这种溶胶凝胶法制备的样品介电层厚度远小于与之前报道的样品,其厚度约为原方法制备样品的25%。在优化操作过程与降低介电层厚度的同时,二氧化锆的介电性质并没有被影响。作者进一步研究了样品的介电特性,在90K到300K之间介电性质的变化小于10%。

英文摘要

In the electronics industry it is desirable to employ materials which allow for low-voltage operation and device designs based on very thin layers. In addition, these materials are supposed to be applicable in an easy, fast and reliable way. In this paper, we report an optimized procedure to deposit thin zirconium dioxide (ZrO2) high-k dielectric layers in an easy, reliable and very quickly applicable way. The processing time was only 10 minutes as compared to previously reported 140 min. with a similar approach. This optimization included also simplifications of processing procedure. For this particular sol-gel method, a reduction of the film thickness of the dielectric layer compared to previously reported films by a factor of 4 was achieved. These processing and thickness improvements were obtained while all required dielectric properties of ZrO2 were preserved. In addition, a thorough temperature dependence study is presented showing that the dielectric properties change by less than 10 % between 90 and 300 K.

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