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论文摘要

截叶铁扫帚提取物的GC-MS分析及羽扇烯酮的定性定量分析

GC-MS analysis of extractives from Lespedeza cuneate and qualitative and quantitative analysis of lupenone

作者:唐超(贵州医科大学);潘年松(遵义医药高等专科学校);罗俊(贵州医科大学)

Author:TANG Chao(Guizhou Medical University);PAN Nian-Song(Zunyi Medical College);LUO Jun(Guizhou Medical University)

收稿日期:2017-04-12          年卷(期)页码:2018,55(3):643-648

期刊名称:四川大学学报: 自然科学版

Journal Name:Journal of Sichuan University (Natural Science Edition)

关键字:截叶铁扫帚;GC-MS;羽扇烯酮;超声醇提法

Key words:Lespedeza cuneate; GC-MS; Lupenone; Ultrasonic alcohol extraction

基金项目:黔科合LH字[2015]7580号;遵社科合[2015]02号;遵医专科合BS2016002

中文摘要

采用乙醇超声提取三个不同月份的截叶铁扫帚,并运用GC MS法分析截叶铁扫帚乙醚供试液的化学成分和羽扇烯酮的相对含量.结果显示从截叶铁扫帚中共检测出61种成分,5月份截叶铁扫帚的成分有42种,8月份有39种,11月份有42种,均主要为烷烃、萜类、芳香类物质,并首次发现截叶铁扫帚中含有羽扇烯酮,测得5月、8月、11月截叶铁扫帚中羽扇烯酮的含量分别为1.734mg/g、2.235mg/g、1.111mg/g.通过比较三个不同月份截叶铁扫帚中的化学成分及其含量,8月份截叶铁扫帚中化学成分种类最少,但羽扇烯酮含量最高.

英文摘要

Components of the Lespedeza cuneate from three different months were extracted by ultrasonic alcohol extraction method, the extractives were dissolved by ether and analyzed by GC MS, and quantitative analysis of lupenone by GC MS. Results showed that 61 components have been detected. Lespedeza cuneate included 42 components in May, 39 components in August and 42 components in November. The mainly include alkane, terpenoid and aromatics. The lupenone was firstly found in Lespedeza cuneate, and the relative contents of lupenone in May, August and November were respectively 1.734mg/g, 2.235mg/g and 1.111mg/g. Through comparison the Lespedeza cuneate constituents and contents of the three different months, the Lespedeza cuneate constituents was the least in August, but the contents of it is the highest.

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