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论文摘要

加速老化对光固化复合树脂色度和显微结构的影响

The influence of acceler ated aging on color and microstructur e of light - cur ing composite r esin

作者:林金莹 姚江武 林昌健

Author:LIN Jinying1, YAO Jiang- wu2, LIN Chang- jian3

收稿日期:2008-06-25          年卷(期)页码:2008,26(03):291-

期刊名称:华西口腔医学杂志

Journal Name:West China Journal of Stomatology

关键字:老化,复合树脂,色差,红外光谱,环境扫描电子显微镜,

Key words:aging,composite resin,color difference,infrared spectrum,environmental scanning electron microscopy,

基金项目:

中文摘要

目的考察加速老化后光固化复合树脂的色度稳定性、表面显微结构和内部化学结构的改变及其相互之间的关系。方法用老化仪加速老化4种光固化复合树脂样本,测量老化24 h和96 h后的色差。用环境扫描电子显微镜和傅里叶变换红外光谱仪分别观察老化前后样本表面的显微结构和化学键的改变。用方差分析法分析老化时间与树脂色度间的交互影响(α=0.05)。结果老化时间与复合树脂类型之间具有交互作用(P

英文摘要

Objective The aim of this investigation was to examine the changes of the color stability, surface microstructure and chemical constitution of light- curing composite resin after accelerated aging, and the relations between them. Methods Four light - curing composite resin were aged in an accelerated aging instrument. The color was measured by CIE L*a*b* with a spectrophotometer after treatment for 24 h and 96 h. And the color differences were calculated. Environmental scanning electron microscopy(ESEM) and Fourier transform infrared spectroscopy (FTIR) spectrometer were used to examine the microstructure and chemical composition of the specimens before and after accelerated aging. The color differences were analyzed statistically by repeated- measures two- way analysis of variance and t- test after aging for 24 h and 96 h. The level of significance was defined as α=0.05. Results The materials demonstrated statistically significant differences in color after aging between the 24 h and 96 h(P

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