期刊导航

论文摘要

不同处理方法对瓷表面微观形貌的影响

Influence of different surface treatments on porcelain surface topography

作者:台银霞 朱宪春 闫森 刘畅 张娴 史学明

Author:Tai Yinxia, Zhu Xianchun, Yan Sen, Liu Chang, Zhang Xian, Shi Xueming

收稿日期:          年卷(期)页码:2013,31(1):57-57-60

期刊名称:华西口腔医学杂志

Journal Name:West China Journal of Stomatology

关键字:表面处理,扫描电子显微镜,氢氟酸,Nd: YAG激光,

Key words:surface treatment,scanning electron microscope,hydrofluoric acid,Nd: YAG laser,

基金项目:

吉林省卫生厅科技计划基金资助项目(2009Z006)

中文摘要

目的 研究不同瓷表面处理方法对瓷表面微观形貌的影响。方法 制备6组金属烤瓷试样,分别在瓷表面进行如下处理:A组不作处理(对照组),B组采用质量分数9.6%氢氟酸(HF)酸蚀,C组用金刚砂车针与HF联合处理, D、E、F组分别用0.75、1.05、1.45 W的Nd: YAG激光与HF联合处理。处理后的试件用扫描电子显微镜(SEM)观察, 观察其表面形貌的变化。结果 经不同处理后瓷表面的微观形貌不同;E组经1.05 W的Nd: YAG激光与HF联合处理,瓷表面可见网格形裂纹,裂纹的侧壁及底部布满类圆形小孔,裂纹内壁圆钝,并且观察到直径约为20 μm的圆形弹坑样结构,其内壁附有直径为1~5 μm不等的圆形隐窝,形成倒凹结构。结论 能量参数为1.05 W的Nd: YAG激光与9.6%HF联合处理瓷面后可使瓷面均匀粗化,是一种有效的瓷表面处理方法。

英文摘要

ObjectiveTo evaluate the influence of different surface treatments on porcelain surface topography.Methods Metal ceramic prostheses in 6 groups were treated according to the different surface treatment methods, and the surface topography was observed through scanning electron microscope(SEM). Group A was the control one (untreated), group B was etched by 9.6% hydrofluoric acid(HF), group C was deglazed by grinding and then etched by 9.6% HF, group D was treated with Nd: YAG laser irradiation(0.75 W) and HF etching, group E was treated with Nd: YAG laser irradiation(1.05 W) and HF etching, and group F was treated with laser irradiation(1.45 W) and HF etching.Results Surface topography was different in different groups. A lot of inerratic cracks with the shapes of rhombuses and grid, and crater with a shape of circle were observed on the ceramic surface after treatment with energy

parameters of 1.05 W Nd: YAG laser irradiation and 9.6% HF etching(group E). Surface topography showed a lot of concaves on the inner wall of the cracks, and the concaves with diameter of 1-5 μm could be observed on the inner wall of the holes, which had a diameter of 20 μm under SEM.ConclusionThe use of Nd: YAG laser irradiation with the energy parameters of 1.05 W and the HF with a concentration of 9.6% can evenly coarsen the porcelain surface, that is an effective surface treatment method.

关闭

Copyright © 2020四川大学期刊社 版权所有.

地址:成都市一环路南一段24号

邮编:610065