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论文摘要

硼化钽(TaB)高温高压烧结体硬度的研究

Studies of the hardness for the sintered tantalum boride (TaB) at high temperature and high pressure

作者:陈海花(青海大学基础部);梁浩(四川大学原子与分子物理研究所);谢名财(青岛大学基础部);刘凌霄(青岛大学基础部);郑曙东(青岛大学基础部)

Author:CHEN Hai-Hua(Foundation Department of Qinghai University);LIANG Hao(Institute of Atomic and Molecular Physics, Sichuan University);XIE Ming-Cai(Foundation Department of Qinghai University);LIU Ling-Xiao(Foundation Department of Qinghai University);ZHENG Shu-Dong(Foundation Department of Qinghai University)

收稿日期:2017-04-09          年卷(期)页码:2017,54(4):835-838

期刊名称:四川大学学报: 自然科学版

Journal Name:Journal of Sichuan University (Natural Science Edition)

关键字:硼化钽;高温高压烧结;硬度;相对密度

Key words:Tantalum boride; HTHP sintering; Vickers hardness; Relative density

基金项目:国家自然科学基金,省自然科学基金

中文摘要

采用国产DS6×800T铰链式六面顶压机技术,对过渡金属TaB粉末进行了高温高压烧结,并采用金刚石菱形压痕法对TaB维氏硬度进行了测量。在加载负荷为29.4 N时,烧结压力为4 GPa,烧结温度分别为900和1100 ℃时,测试得到TaB陶瓷的硬度分别为7.7±0.4和 10.5±0.7 GPa。说明在同一压力条件下,温度越高致密性越好,通过阿基米德法,计算得到了TaB的相对密度为13.5 g/cm3。

英文摘要

Tantalum boride has been sintered under high temperature and high pressure (HTHP) conditions by using a DS6×8 MN cubic press device, and the Vickers hardness of TaB has been measured by using a diamond indentation method. Under the applied load of 29.4 N, our test gave the Vickers hardness of TaB are 7.7±0.4 and 10.5±0.7 GPa, at 4 GPa and the temperatures of 900 and 1100 ℃, respectively. Our result shows that the density becomes better with the increasing temperature under the same pressure. By using the Archimedes method, we calculated the relative density of 13.5 g/cm3 for TaB.

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