β-氯乙基-3-O-雌酚酮醚合成方法改进
IMPROVED SYNTHESIS OF β-CHLOROETHYL-3-O-ESTRONE ETHER
作者:李灵芝,郑虎
Author:
收稿日期: 年卷(期)页码:1998,(02):-105-111
期刊名称:华西药学杂志
Journal Name:WEST CHINA JOURNAL OF PHARMACEUTICAL SCIENCES
关键字:雌酚酮;相转移反应
Key words:
基金项目:
中文摘要
采用1,2-二氯乙烷既作溶剂,又作烃化剂,50%NaOH作碱,经相转移反应,一步制得定量收率产物,产品纯度高,无需重结晶。
参考文献
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