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论文摘要

甲基丙烯酰氧基丙基三甲氧基硅烷对3种不同金属与Filtek树脂粘接强度的影响

The influence of methacryloxy propyl trimethoxyl silane on shear bond strength of three kinds metal and Filtek resin

作者:王建鸿1 黄辉2 章福保1 石连水1 朱洪水1

Author:Wang Jianhong1, Huang Hui2, Zhang Fubao1, Shi Lianshui1, Zhu Hongshui1.

收稿日期:2011-06-13          年卷(期)页码:2012,30(5):535-535-538

期刊名称:华西口腔医学杂志

Journal Name:West China Journal of Stomatology

关键字:偶联剂, 镍铬合金, 钛, 金钯合金, 树脂, 粘接, 剪切强度,

Key words:primer coupling agent, nickel-chromium alloy, titanium, aurum-palladium alloy, resin, adhesion, shear bond resistance,

基金项目:

江西省科技厅基金资助项目(20061c0600900)

中文摘要

目的研究经甲基丙烯酰氧基丙基三甲氧基硅烷(γ-MPS)偶联剂处理的3种不同金属的粘接表面对FiltekZ350树脂粘接强度的影响。方法用失蜡铸造法制备镍铬合金、纯钛、金钯合金试件各12个,共36个。每种金属随机平分为实验组和对照组,每组6个。实验组用γ-MPS对粘接面进行处理后与Filtek Z350树脂粘接,对照组粘接面不用γ-MPS处理。测试每组试件断裂时的剪切力,并用扫描电子显微镜(SEM)观察试件断面的形貌。结果镍铬合金实验组、纯钛实验组较相应对照组的剪切强度高,差异有统计学意义(P0.05)。实验组内比较:纯钛组剪切强度高于镍铬合金组,两者又均高于金钯合金组(P

英文摘要

Objective To study the influence of three different metal alloy surfaces treated with primer methacryloxy propyl trimethoxyl silane(γ-MPS) coupling agent on the bond strength of Filtek Z350 resin. Methods Total 36 specimens of nickel-chromium(Ni-Cr) alloy, pure titanium(Ti) and aurum-palladium(Au-Pd) alloy, each of 12 pieces produced by lost wax casting method, were divided into 6 groups. After treated with γ-MPS on the bonding surface, experimental group samples were adhered to Filtek Z350 resin, then compared with the surface without γ-MPS treatment. The tensile and shear strength of each group tested and the fracture sections were observed with scanning electron microscope(SEM). Results Comparing the Ni-Cr alloy and pure Ti experimental group with them in control

group, the shearing strength of the experimental group was higher, and the differences were significant(P0.05). Comparing the experimental groups, the shearing strength of pure Ti was higher than Ni-Cr alloy, both were higher than Au-Pd alloy(PTi experimental group showed more resin juts in the fracture surface, while the Au-Pd alloy in experimental group showed less resin juts. Conclusion γ-MPS can enhance the adhesion between metal and resin, but it is also related to the metal composition. γ-MPS can significantly increase the bond strength of resin and Ti or Ni-Cr alloy, but not the case of Au-Pd alloy and resin.

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