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论文摘要

钛表面预处理对钛—瓷剪切结合强度影响的研究

The Influence of Surface Conditioning on the Shear Bond Strength of La-Porcelain and Titanium

作者:莫安春,岑远坤,廖运茂,王建华

Author:MOAnchun*,CEN Yuankun,LIAO Yunmao,et al.

收稿日期:2003-04-25          年卷(期)页码:2003,21(02):104-

期刊名称:华西口腔医学杂志

Journal Name:West China Journal of Stomatology

关键字:纯钛,牙科陶瓷,钛—瓷界面,

Key words:pure titanium,dental porcelain,porcelain-titanium interface,

基金项目:

中文摘要

目的 探讨不同的钛表面预处理对自制新型镧系低熔瓷的钛—瓷结合强度的影响,为自行研制钛瓷瓷粉体的临床应用奠定理论基础。方法 钛表面分别经不同粒度的Al2O3喷砂粗化、偶联剂处理及预氧化处理;制作棒、盘试件,用压出法测试钛—瓷间的剪切结合强度,用扫描电子显微镜(SEM)及电子探针(EPMA),从微观和相关元素方面观察钛—瓷界面。结果 80~250μm 5种不同粒度的Al2O3喷砂处理钛表面后,对钛—瓷剪切结合强度无明显影响;自制硅偶联剂使剪切结合强度降低;钛表面预氧处理对剪切结合强度无明显影响。结论 镧系低熔瓷对钛表面具有良好的湿润性;钛金属表面硅偶联剂处理或预氧化处理是不必要的;在一定范围内,剪切结合强度受钛表面粗糙度的影响较小。

英文摘要

Objective To determine the influence of different surface conditioning methods on bonding strength of low fusing porcelain (La-Porcelain) and titanium.Methods The surface of the sampleswere sandblasted for 2 minwith 80~250μm Al2O3or coated fortwotimeswith Si-couple agent or conditioned by pre-oxidation. The shear bond strengthwas examined by push- type shear test with a speed of 0·5 mm/min in a universal testing machine. Scanning electron microscopy (SEM) and electron probe micro-analyzer (EPMA) were employed to explore the relationship between bonding strength and microstructures, aswell as the element diffusion at the interface between porcelain coating and titanium when heated at 800℃.Results Bonding strength was not statistically different (P>0·05) after sandblastingwith Al2O3in particle size ranged from 80μm to 250μm. When a Si- couple agent was used, bond of porcelain to titaniumwas significantly lower (P0·05). The SEMresults revealed integrity of porcelain and titanium.Conclusion La-Porcelain showed a small effect of surface coarseness. Sandblastingthe titanium surfacewith 150~ 180μm Al2O3can be recommended as a method for better bonding between La-Porcelain and titanium. The Si-couple agent coating and pre-oxidation of titanium surface is unnecessary.

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