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论文摘要

着色剂对口腔修复用钇稳定氧化锆 陶瓷粉体制备的影响

Effects of colorants on yttria stabilized tetragonal zirconia polycrystals powder

作者:王博 陈剑锋 张言春 王如

Author:Wang Bo, Chen Jianfeng, Zhang Yanchun, Wang Ru.

收稿日期:2015-02-05          年卷(期)页码:2015,33(5):462-462-465

期刊名称:华西口腔医学杂志

Journal Name:West China Journal of Stomatology

关键字:钇稳定氧化锆陶瓷,着色氧化锆,激光粒度分析,

Key words:yttria stabilized tetragonal zirconia polycrystals,colored zirconia,laser particle size analyzer,

基金项目:

国家自然科学基金面上项目(51472270)

中文摘要

目的 探讨着色剂氧化铁(Fe2O3)、氧化铈(CeO2)对口腔修复用钇稳定氧化锆陶瓷(Y-TZP)制备粉体的影响。方法 按照一定比例将口腔修复用Y-TZP粉体和着色剂(Fe2O3 0.15%或CeO2 4%)分别混合,配置成具有一定固含量的Y-TZP喷雾干燥浆料。通过喷雾造粒的方法进行着色和未着色Y-TZP粉体造粒。粉体分成3组,分别为未着色Y-TZP组、0.15%Fe2O3着色Y-TZP组、4%CeO2着色Y-TZP组,分别利用激光粒度分析仪和光学显微镜进行3组粉体粒径和形貌的测量和分析。结果 3组口腔修复用Y-TZP造粒粉体的颗粒D50总体均数差异有统计学意义(P0.05)。Fe2O3、CeO2作为Y-TZP的内着色剂,粉体大多成球形。结论 CeO2作为口腔修复用Y-TZP的着色剂,对造粒粉料的粒径分布以及成球性能影响不大;Fe2O3作为着色剂进行内着色对颗粒的粒径产生一定的影响。

英文摘要

Objective To evaluate the effect of Fe2O3 and CeO2 as colorants on yttria stabilized tetragonal zirconia polycrystals (Y-TZP) powder.Methods The spray granulation slurry of colored zirconia was prepared with different concentrations of Fe2O3 (0.15%) and CeO2 (4%), which were added in Y-TZP. Zirconia powder was made by spray granulation. The powder specimens were divided into three groups: uncolored zirconia, Fe2O3 (0.15%) zirconia, and CeO2 (4%) zirconia. The particle morphologies of the powder specimens were measured with a laser particle size analyzer and an optical microscope.Results The differences in D50 among the three groups were statistically significant (P0.05). Mostly spherical powder was observed in the three groups.Conclusion Fe2O3 as a colorant can affect particles, whereas CeO2 has no effect.

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