期刊导航

论文摘要

微波烧结和常规烧结对牙科用氧化锆半透性影响的对比研究

Translucency of dental zirconia ceramics sintered in conventional and microwave ovens

作者:江月梅,杨瑛,詹文辉,胡国新,杨秋霞

Author:Jiang Yuemei, Yang Ying, Zhan Wenhui, Hu Guoxin, Yang Qiuxia

收稿日期:2015-05-18          年卷(期)页码:2015,33(6):642-642-645

期刊名称:华西口腔医学杂志

Journal Name:West China Journal of Stomatology

关键字:氧化锆,微波烧结,半透性,常规烧结,显微结构,

Key words:zirconia,microwave sintering,translucency,conventional sintering,microstructure,

基金项目:

中文摘要

目的 研究微波烧结对氧化锆半透性的影响并与常规烧结对比,分析半透性与显微结构的相关性。方法 选取Lava和Zenostar两种品牌氧化锆试件各10个,每组5个试件,常规烧结组温度分别为1 500 ℃和1 490 ℃,保温2 h;微波烧结组均以15 ℃·min-1升温至1 420 ℃,保温30 min。用ShadeEye NCC电脑比色仪测量各试件在白背景下和黑背景下的明度的分级(L*)、红到绿两色相极的变化(a*)、黄到蓝两色相极的变化(b*)值,并计算半透性参数(TP),阿基米德排水法测量各试件的密度,扫描电镜(SEM)观察各试件的显微结构。结果 与常规烧结相比,微波烧结Lava和Zenostar氧化锆晶粒尺寸小且均匀一致,密度和TP值虽较高,但差异并无统计学意义(P>0.05)。Lava氧化锆的TP值大于Zenostar氧化锆(P

英文摘要

Objective To evaluate the effect of microwave sintering on the translucency of zirconia and to compare these effect with those of conventional sintering. The relationship between the microstructure of specimens and translucency was investigated. Methods A total of 10 disc-shaped specimens were fabricated from 2 commercial brands of zirconia, namely, Zenostar and Lava. Each group included 5 discs. Conventional sintering was performed according to the manufacturers’ specifications. The maximum temperature for Zenostar was 1 490 ℃, whereas that for Lava was 1 500 ℃. The dwelling time was 2 h. The sintering temperature for microwave sintering was 1 420 ℃, heating rate was 15 ℃·min-1, and dwelling time was 30 min. After sintering, the translucency parameter (TP) of the specimens were measured with ShadeEye NCC. The sintered density of the specimens was determined by Archimedes’ method. The grain size and microstructure of the specimens were investigated by scanning electron microscopy. Results Density and translucency slightly increased by microwave sintering, but no significant difference was found between microwave and conventional sintering (P>0.05). Small and uniform microstructure were obtained from microwave sintering. The mean TP of Lava was significantly higher than that of Zenostar (P

关闭

Copyright © 2020四川大学期刊社 版权所有.

地址:成都市一环路南一段24号

邮编:610065