期刊导航

论文摘要

两种表面处理方法对改良型聚醚醚酮弯曲强度的影响

Effect of two kinds of surface pretreatments on bending strength to the modified polyetheretherketone

作者:何光霁,张文云

Author:Guangji He,Wenyun Zhang

收稿日期:2018-07-22          年卷(期)页码:2019,37(4):384-384-388

期刊名称:华西口腔医学杂志

Journal Name:West China Journal of Stomatology

关键字:聚醚醚酮,表面处理,弯曲强度,

Key words:polyetheretherketone,surface treatment,bending strength,

基金项目:

中文摘要

目的 通过三点弯曲试验,评价表面喷砂及酸蚀处理对改良型聚醚醚酮(PEEK)强度的影响。方法 制作15 mm×2 mm×1 mm的改良型PEEK(BioHPP)试件48个,随机分为A~H组,A、B、C组喷砂压力均为0.2 MPa,喷砂粒度依次为120、50、250 μm;D组则在0.7 MPa压力下120 μm粒径喷砂;E、F、G组分别采用98%浓硫酸酸蚀60、120、300 s,H组(对照组)不进行任何表面处理。处理完成后,从各组中随机抽取一个试件用扫描电镜(SEM)观察其表面形貌,其余试件则进行三点弯曲强度测试。采用SPSS 22.0软件对实验数据进行统计分析,检验其差异是否具有统计学意义。结果 SEM观察结果表明,处理后试件表面形貌发生了变化,呈现出不同程度的裂隙、凹坑或孔洞。通过三点弯曲测试发现,与对照组相比,经喷砂或浓硫酸处理后试件强度均有所下降(PP>0.05);相同粒度下,D组试件的强度低于A组(PP>0.05)。结论 表面喷砂或浓硫酸酸蚀均会使BioHPP的弯曲强度显著下降,其强度会随着喷砂的压力增加而明显下降,但不会随着喷砂粒径大小及酸蚀时长变化而发生显著的改变。

英文摘要

ObjectiveTo evaluate the effect of sandblasting or acid etching on the three-point bending strength to the modified polyetheretherketone (PEEK).MethodsForty-eight bars (15 mm×2 mm×1 mm) of specimens were fabricated from the modified PEEK (BioHPP). They were randomly divided into the following groups: A, B, C and D groups, which were blasted with alumina particles; E, F, and G groups, which were etched with 98% concentrated sulfuric acid; and control group H. The sand blast pressure of groups A, B and C was 0.2 MPa, and the grain sizes of the sand blasted were 120, 50, and 250 μm, respectively. Group D was blasted with 120 μm particle size at 0.7 MPa pressure. Groups E, F and G were acid etched for 60, 120, and 300 s, respectively. No surface treatment was conducted in group H. After all the specimens were processed, one sample was randomly selected from each group to observe its surface morphology under a scanning electron microscope (SEM), and the other specimens were tested for their three-point bending strength. SPSS 22.0 software was used to analyze the experimental data and to test whether the difference was statistically significant.ResultsSEM observation showed that the surface morphology of the specimen changed after the treatment and revealed different degrees of cracks, pits, or voids. The three-point bending test indicated that the strength of the specimens treated with sandblasting or concentrated sulfuric acid decreased compared with that of the control group (PP>0.05). The strength of group D was lower than that of group A at the same particle size (PP>0.05).ConclusionThe bending strength of BioHPP could be significantly decreased by surface sand blasting or concentrated sulfate etching as the sandblasting pressure increased, but the bending strength did not decrease as sand particle size and acid etching time changed.

下一条:替牙列期口呼吸儿童腭部形态的三维分析

关闭

Copyright © 2020四川大学期刊社 版权所有.

地址:成都市一环路南一段24号

邮编:610065